How Do You Prepare Glacial Acetic Acid For Making N Butyl Acetate?
The best is to buy acetic acid labeled glacial from a supplier. Making it is a pain. To make it, you would freeze acetic acid. Pure acetic acid freezes at 40C, 104F. You freeze it to the point where you have frozen slush in liquid acid. Working always in the cold, decant or filter the slush away from the liquid. Melt the slush and refreeze.